Dichlorine hexoxide

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Dichlorine hexoxide
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Molar mass 166.901 g/mol
Appearance red liquid
Density 1.65 g/cm3
Melting point Template:Chembox CalcTemperatures
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Dichlorine hexoxide is the chemical compound with the molecular formula Template:Chem2 or Template:Chem2, which is correct for its gaseous state. However, in liquid or solid form, this chlorine oxide ionizes into the dark red ionic compound chloryl perchlorate or dioxochloronium(V) perchlorate Template:Chem2, which may be thought of as the mixed anhydride of chloric and perchloric acids. This compound is a notable perchlorating agent.[1]

It is produced by reaction between chlorine dioxide and excess ozone:

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Molecular structure

It was originally reported to exist as the monomeric chlorine trioxide Template:Chem2 in gas phase,[2] but was later shown to remain an oxygen-bridged dimer after evaporation and until thermal decomposition into chlorine perchlorate, Template:Chem2, and oxygen.[3] The compound Template:Chem2 was then rediscovered.[4]

It is a dark red fuming liquid at room temperature that crystallizes as a red ionic compound, chloryl perchlorate, Template:Chem2. The red color shows the presence of chloryl ions. Thus, chlorine's formal oxidation state in this compound remains a mixture of chlorine(V) and chlorine(VII) both in the gas phase and when condensed; however by breaking one oxygen-chlorine bond some electron density does shifts towards the chlorine(VII).

Properties

Template:Chem2 is diamagnetic and is a very strong oxidizing agent. Although stable at room temperature, it explodes violently on contact with organic compounds[5] It is a strong dehydrating agent:

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Many reactions involving Template:Chem2 reflect its ionic structure, Template:Chem2, including the following:[6]

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It reacts with gold to produce the chloryl salt [[chloryl tetraperchloratoaurate|Template:Chem2]]:[7]

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Several other transition metal perchlorate complexes are prepared using dichlorine hexoxide.

Nevertheless, it can also react as a source of the Template:Chem2 radical:Script error: No such module "Unsubst".

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Synthesis

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References

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