Yttrium(III) chloride

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Yttrium(III) chloride
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Template:Longitem YCl3
Molar mass 195.265 g/mol[1]
Appearance white solid
Density 2.61 g/cm3[1]
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Solubility 601 g/L ethanol (15 °C)
606 g/L pyridine (15 °C)[2]
Template:Longitem Monoclinic, mS16
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a = 0.692 nm, b = 1.194 nm, c = 0.644 nm
α = 90°, β = 111°, γ = 90°
Template:Longitem Yttrium(III) fluoride
Yttrium(III) bromide
Yttrium(III) iodide
Template:Longitem Scandium(III) chloride
Lutetium(III) chloride

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Yttrium(III) chloride is an inorganic compound of yttrium and chloride. It exists in two forms, the hydrate (YCl3(H2O)6) and an anhydrous form (YCl3). Both are colourless salts that are highly soluble in water and deliquescent.

Structure

Solid YCl3 adopts a cubicScript error: No such module "Unsubst". structure with close-packed chloride ions and yttrium ions filling one third of the octahedral holes and the resulting YCl6 octahedra sharing three edges with adjacent octahedra, giving it a layered structure.[3][4] This structure is shared by a range of compounds, notably AlCl3.

Preparation and reactions

YCl3 is often prepared by the "ammonium chloride route," starting from either Y2O3 or hydrated chloride or oxychloride.[5][6] or YCl3·6H2O.[7] These methods produce (NH4)2[YCl5]:

10 NH4Cl + Y2O3 → 2 (NH4)2[YCl5] + 6 NH3 + 3 H2O
YCl3·6H2O + 2 NH4Cl → (NH4)2[YCl5] + 6 H2O

The pentachloride decomposes thermally according to the following equation:

(NH4)2[YCl5] → 2 NH4Cl + YCl3

The thermolysis reaction proceeds via the intermediacy of (NH4)[Y2Cl7].

Treating Y2O3 with aqueous HCl produces the hydrated chloride (YCl3·6H2O). When heated, this salt yields yttrium oxychloride rather than reverting to the anhydrous form.

References

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  3. Wells A.F. (1984) Structural Inorganic Chemistry 5th edition Oxford Science Publications Template:ISBN
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